HRID1627235

反应详情

EQUATION

反应方程式

HRID 1627235 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
50 °C

PROCEDURE

实验过程

To a solution of KOH (1.12 g) in 10 ml of demineralised water, Nicotinic acid was added and stirred well at 50° C. for 3 h. Water was removed in a rotavapour. The solid was dried under vacuum at 120° C. to remove final traces of water to give 3.1 g of white solid with m.pt >325° C.

WORKUP

后处理

  1. customWater was removed in a rotavapour
  2. customThe solid was dried under vacuum at 120° C.
  3. customto remove final traces of water