HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 1-aminocyclohexane-1-carboxylate hydrochloride → HCID 57672866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 1-aminocyclohexane-1-carboxylate hydrochloride | HCID 11241228 | — |
| Reactant | HCID 67181841 | HCID 67181841 | — |
| Product | HCID 57672866 | HCID 57672866 | 65% |
Reaction Steps
741 mg (3.57 mmol) of 1-aminocyclohexanecarboxylic acid ethyl ester hydrochloride was used instead of 1-aminocyclohexanecarboxylic acid methyl ester hydrochloride and 1.00 g (3.57 mmol) of 4-(4-propylpiperazin-1-yl)benzoic acid hydrochloride was used instead of 3-furancarboxylic acid in the process according to Reference Example 15 to obtain 928 mg (65%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785631B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-c24e7d78c1ec40478488a80097ab03d2 |
| Source note | uspto-grants-2014_07 |