HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethylaniline → HCID 67215826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethylaniline | HCID 6896 | — |
| Reactant | 3-Bromotoluene | HCID 11560 | — |
| Product | HCID 67215826 | HCID 67215826 | 93% |
Reaction Steps
Following the general procedure using 3-bromotoluene (121 μL, 1.00 mmol) and 2,6-dimethylaniline (148 μL, 1.20 mmol), the reaction was stirred for 19 h at rt. Column chromatography on silica gel (eluting with 30% EtOAc/hexanes) afforded the product as an off-white solid (196 mg, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-fc2816dd830e4db98a9737c6142dac70 |
| Source note | uspto-grants-2014_07 |