HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylamine → (E)-N,N-Dibenzyl-3-phenylprop-2-en-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylamine | HCID 7656 | — |
| Reactant | Cinnamyloxybenzene | HCID 258010 | — |
| Product | (E)-N,N-Dibenzyl-3-phenylprop-2-en-1-amine | HCID 9944644 | 93% |
Reaction Steps
Following the general procedure using cinnamyloxybenzene (105 mg, 0.50 mmol) and dibenzylamine (148 mg, 0.75 mmol), the reaction was stirred for 0.5 h at rt. Column chromatography on silica gel (eluting with 8% EtOAc/hexanes) afforded the product as a pale yellow liquid (145 mg, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08785665B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-9d99684539ab40b09f64d2b6f5687328 |
| Source note | uspto-grants-2014_07 |