HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphate → 2,4-Diphenyl-6-(4'-vinylbiphenyl-3-yl)-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphate | HCID 1061 | — |
| Reactant | 4-Vinylphenylboronic acid | HCID 2734393 | — |
| Reactant | 2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine | HCID 58943302 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Sodium Carbonate | HCID 10340 | — |
| Product | 2,4-Diphenyl-6-(4'-vinylbiphenyl-3-yl)-1,3,5-triazine | HCID 68359056 | — |
Reaction Steps
1.16 g (0.003 mol) of 2-(3-bromophenyl)-4,6-diphenyl-1,3,5-triazine, 0.74 g (0.005 mol) of 4-styreneboronic acid and 0.023 g (0.02 mmol) of tetrakispalladium phosphate are stirred under reflux for 24 h in 45 ml of THF and 30 ml of 1M sodium carbonate solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08786181B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-cbf93174ce744d0bbe2f22044b5bd425 |
| Source note | uspto-grants-2014_07 |