Methyl 4-amino-3-methylbenzoate → HCID 67048451, compound

HRID 1629870Notes

Reaction equation

HRID 1629870 reaction equation
[NH2:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:4][C:3]=1[CH3:12].[Cl:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][S:19](Cl)(=[O:21])=[O:20]>N1C=CC=CC=1>[Cl:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][S:19]([NH:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:4][C:3]=1[CH3:12])(=[O:21])=[O:20]

Participants

4

Reactant 2

HCID 2736799Methyl 4-amino-3-methylbenzoateHCID 12589202HCID 12589202, compound

Product 1

HCID 67048451HCID 67048451, compoundYield 43%

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Prepared analogously to Example 83a from methyl 4-amino-3-methyl-benzoate and 5-chloropentyl-sulphonic acid chloride in pyridine. Yield: 43%

Sources & evidence

ORD record
ord-05d5dc50485348c38ddd5bcc345ad303
Source dataset
uspto-grants-2014_07
Patent number
US08791103B2

Reaction notes

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