HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4,5-Trimethoxyaniline → HCID 59343474, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4,5-Trimethoxyaniline | HCID 32285 | — |
| Edukt | 2-Chloro-6-(3-phenyl-phenyl-oxy)-pyrazine | HCID 59343501 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | HCID 59343474 | HCID 59343474 | 78% |
Reaktionsschritte
Using Method EE (reaction time: 4 hours) with 2-chloro-6-[(3-phenyl)-phenyl-oxy]-pyrazine (100 mg, 0.35 mmol) and 3,4,5-trimethoxyaniline (84 mg, 0.46 mmol), and purification by column chromatography (AcOEt), the title compound was obtained (117 mg). Yield: 78%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07737152B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-335e1fdb52e8459d8d545c88612a6a00 |
| Quellennotiz | uspto-grants-2010_06 |