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HRID1630406

反应详情

EQUATION

反应方程式

HRID 1630406 的结构方程式

REACTANTS

反应物

2
结构：O=CC=P(c1ccccc1)(c1ccccc1)c1ccccc1
HCID75051

(Triphenylphosphoranylidene)acetaldehyde

C20H17OP

结构：O=Cc1ccc(-c2cccc(F)c2)cn1
HCID46313112

5-(3-Fluorophenyl)-2-pyridinecarboxaldehyde

C12H8FNO

PRODUCTS

生成物

1
结构：O=C/C=C/c1ccc(-c2cccc(F)c2)cn1
HCID86676729

未命名化合物

PROCEDURE

实验过程

584 mg of 5-(3-fluorophenyl)pyridine-2-carbaldehyde and 883 mg of (triphenylphosphoranylidene)acetaldehyde are stirred at RT overnight. The solvent is evaporated and the residue is purified by column chromatography (silica gel, MeOH:DCM=99.5:0.5).

WORKUP

后处理

  1. customThe solvent is evaporated
  2. customthe residue is purified by column chromatography (silica gel, MeOH:DCM=99.5:0.5)