Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1630439Generated: October 29, 2026

Trichloroacetic Acid → HCID 57954477, compound

https://huagongshe.com/reaction/1630439

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrichloroacetic AcidHCID 6421—
ReactantN-(oxan-4-ylidene)hydroxylamineHCID 12298558—
ReactantHCID 178418268HCID 178418268—
ProductHCID 57954477HCID 57954477—

Reaction Steps

4-Nitrosotetrahydro-2H-pyran-4-yl 2,2,2-trichloroacetate was prepared from tetrahydro-pyran-4-one oxime, lead tetraacetate and trichloroacetic acid using conditions of General Method 3. 1H NMR (360 MHz, chloroform-d) δ 3.99-4.19 (2H, m), 3.61-3.94 (2H, m), 2.30-2.61 (2H, m), 1.58-2.03 (2H, m).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08791134B2
Source datasetuspto-grants-2014_07
ORD IDord-7cdc57b4c88b4940997805f9cc5db38e
Source noteuspto-grants-2014_07