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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1630440Generated: October 31, 2026

Pentafluoropropionic acid → HCID 57954506, compound

https://huagongshe.com/reaction/1630440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPentafluoropropionic acidHCID 62356—
ReactantN-(oxan-4-ylidene)hydroxylamineHCID 12298558—
ReactantHCID 178418268HCID 178418268—
ProductHCID 57954506HCID 57954506—

Reaction Steps

4-Nitrosotetrahydro-2H-pyran-4-yl 2,2,3,3,3-pentafluoropropanoate was prepared from tetrahydro-pyran-4-one oxime, lead tetraacetate and pentafluoropropionic acid using conditions of General Method 3. 1H NMR (250 MHz, chloroform-d) δ 4.11-4.30 (2H, m), 3.46-3.83 (2H, m), 2.45-2.73 (2H, m), 1.68-2.02 (2H, m).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08791134B2
Source datasetuspto-grants-2014_07
ORD IDord-e73060f2abda4e019a674ace3466e430
Source noteuspto-grants-2014_07