HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperidin-4-one oxime → Dibutyl 1-methyl-4-nitrosopiperidin-4-yl phosphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperidin-4-one oxime | HCID 339053 | — |
| Reactant | Dibutyl phosphate anion | HCID 3790919 | — |
| Reactant | HCID 178418268 | HCID 178418268 | — |
| Product | Dibutyl 1-methyl-4-nitrosopiperidin-4-yl phosphate | HCID 57954472 | — |
Reaction Steps
Dibutyl 1-methyl-4-nitrosopiperidin-4-yl phosphate was prepared from 1-methyl-piperidin-4-one oxime, lead tetraacetate and dibutyl phosphate using conditions of General Method 3. 1H NMR (360 MHz, chloroform-d) δ 4.03-4.17 (4H, m), 2.77-2.88 (2H, m), 2.27-2.40 (6H, m), 2.12-2.24 (4H, m), 1.59-1.83 (6H, m), 1.38 (4H, q, 7.2 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08791134B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d66f9610286443bd9b81dc06709a5987 |
| Source note | uspto-grants-2014_07 |