Methyl 4-bromo-3-(methoxymethyl)benzoate → HCID 46908811, compound

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Reaction Steps

The title compound was prepared following procedure described in Method B starting from Intermediate A1 and 6-(dimethylamino)-N′-hydroxypyridine-3-carboximidamide (UkrOrgSynthesis, BBV-073023). After purification by flash chromatography (silica, EtOAc/cHex) followed by a crystallization from a hot mixture of MTBE and heptane, the title compound was obtained as a white powder. HPLC (Method A), Rt: 4.0 min (purity: 100%). UPLC/MS, M+(ESI): 401.1. Elemental analysis: [C24H24N4O2-0.1H20] calculated: C, 71.66%; H, 6.06%; N, 13.93%. found: C, 71.66%; H, 6.06%; N, 13.91%.

Provenance & Evidence