Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Benzofuran-2-sulfonyl chloride → N-(5-chloro-2-{[(5-nitro-1H-pyrazol-3-yl)methyl]thio}phenyl)-1-benzofuran-2-sulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Benzofuran-2-sulfonyl chloride | HCID 2795172 | — |
| 반응물 | 5-chloro-2-(((5-nitro-1H-pyrazol-3-yl)methyl)thio)aniline | HCID 136372389 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | N-(5-chloro-2-{[(5-nitro-1H-pyrazol-3-yl)methyl]thio}phenyl)-1-benzofuran-2-sulfonamide | HCID 136372390 | 71% |
반응 단계
Following General Procedure B, the title compound (580 mg, 71%) was prepared from 5-chloro-2-(((5-nitro-1H-pyrazol-3-yl)methyl)thio)aniline (503 mg, 1.77 mmol) and benzofuran-2-sulfonyl chloride (384 mg, 1.77 mmol) in pyridine (5 ml).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08791161B2 |
| 출처 데이터셋 | uspto-grants-2014_07 |
| ORD ID | ord-4cc256e475934f919d53e8364a15ddfa |
| 출처 메모 | uspto-grants-2014_07 |