Sodium Bicarbonate → HCID 67284761, compound

Participants

Reaction Steps

2-[2,6-Bis(4-pyridylethynyl)phenoxy]ethyl 2,3,4,6-tetra-O-acetyl-D-glucopyranoside (600 mg, 0.895 mmol) and a methanol (90 ml) solution of sodium methoxide (242 mg, 4.47 mmol) were stirred at room temperature for 12 hours. The reaction mixture was neutralized with a sodium hydrogen carbonate aqueous solution, and concentrated under reduced pressure. The residue was washed with water, and dried to obtain 391 mg of the target product as a white solid (yield: 87%).

Provenance & Evidence