HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethenylbenzenesulfonamide → N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethenylbenzenesulfonamide | HCID 11367403 | — |
| Reactant | 2,4-Dichloro-6-isocyanato-1,3,5-triazine | HCID 13052624 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide | HCID 20218271 | — |
Reaction Steps
A solution of 4,6-dichloro-1,3,5-triazin-2-yl isocyanate (0.87 g, 4.5 mmol) in acetonitrile (9 ml) is contacted with 2-ethenylbenzenesulfonamide (0.83 g, 4.5 mmol) and stirred for 16 hours. The mixture is then evaporated under reduced pressure to yield the title compound which is used directly in subsequent reactions.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474601 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-f1efcf3176904dcab7a8abb854cd9628 |
| Source note | uspto-grants-1984_10 |