HCID 13520103, compound → HCID 20135757, compound

HRID 1632305Notes

Reaction equation

HRID 1632305 reaction equation
[CH3:1][CH:2]([N:6]([CH2:9][CH3:10])[CH2:7][CH3:8])[CH2:3][CH2:4][Br:5].S(C1C=CC(C)=CC=1)(O[CH2:15][CH:16](C)[CH2:17]CCCOC1C=CC=CC=1)(=O)=O>>[BrH:5].[CH2:1]([CH:2]([N:6]([CH2:9][CH3:10])[CH2:7][CH3:8])[CH2:3][CH2:4][Br:5])[CH:16]([CH3:17])[CH3:15]

Participants

3

Reactant 2

HCID 13520103HCID 13520103, compoundHCID 20135827HCID 20135827, compound

Product 1

HCID 20135757HCID 20135757, compoundYield 75%

Procedure

The procedures of preparing 1-methyl-3-bromopropyldiethylamine as described above were repeated except that 11.31 g of 2-methyl-6-phenoxyhexyl tosylate was employed instead of the 10 g of 4-phenoxy-2-butyl tosylate, and 5.33 g of 1-isobutyl-3-bromopropyldiethylamine hydrobromide was obtained in a yield of 75%.

Sources & evidence

ORD record
ord-032fb7e7cbc848cebd835919478d9858
Source dataset
uspto-grants-1984_10
Patent number
US04474964

Reaction notes

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