HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxide (P4O10) → HCID 20444567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | HCID 20444572 | HCID 20444572 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20444567 | HCID 20444567 | — |
Reaction Steps
Into a 500 ml flask equipped with stirrer, dripping funnel and reflux condenser, there were introduced 12 g of P2O5 in 250 ml of methylene-chloride (CH2Cl2), then dropwise and under stirring, a solution of 10.8 g of 5,7,7,7-tetrachloro-2-methyl-heptan-3-ol (see Example 6) in 50 ml of CH2Cl2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04474980 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-1319fbd4b8e842fbae2f0a1f79931d6b |
| Source note | uspto-grants-1984_10 |