Z-Ala-gln-OH → L-Alanyl-L-Glutamine

HRID 1632385Notes

Reaction equation

HRID 1632385 reaction equation
[NH:1](C(OCC1C=CC=CC=1)=O)[C@H:2]([C:4]([NH:6][C@H:7]([C:13]([OH:15])=[O:14])[CH2:8][CH2:9][C:10](=[O:12])[NH2:11])=[O:5])[CH3:3]>O.CO.[Pd]>[NH2:1][C@H:2]([C:4]([NH:6][C@H:7]([C:13]([OH:15])=[O:14])[CH2:8][CH2:9][C:10](=[O:12])[NH2:11])=[O:5])[CH3:3]

Participants

5

Reactant 1

HCID 14534789Z-Ala-gln-OH

Product 1

HCID 123935L-Alanyl-L-Glutamine

Reagents, catalysts & solvents 3

HCID 23938PalladiumCatalystHCID 887MethanolSolventHCID 962WaterSolvent

Procedure

3.50 Grams of Z-Ala-Gln-OH was dissolved in 50 ml of water and 30 ml of methanol, and the mixture was catalytically reduced by using palladium as a catalyst to obtain H-Ala-Gln-OH.

Sources & evidence

ORD record
ord-43374a33a66641a7a69e2881009e5b02
Source dataset
uspto-grants-1984_10
Patent number
US04474754

Reaction notes

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