HCID 101282742, compound → Hydrazinecarboxylic acid, 2-(2,5-diamino-1,5-dioxopentyl)-, 1,1-dimethylethyl ester, (S)-

HRID 1632397Notes

Reaction equation

HRID 1632397 reaction equation
[NH:1](C(OCC1C=CC=CC=1)=O)[C@H:2]([C:8]([NH:10][NH:11][C:12]([O:14][C:15]([CH3:18])([CH3:17])[CH3:16])=[O:13])=[O:9])[CH2:3][CH2:4][C:5](=[O:7])[NH2:6]>CO.[Pd]>[NH2:1][C@H:2]([C:8]([NH:10][NH:11][C:12]([O:14][C:15]([CH3:18])([CH3:17])[CH3:16])=[O:13])=[O:9])[CH2:3][CH2:4][C:5](=[O:7])[NH2:6]

Participants

4

Reactant 1

HCID 101282742HCID 101282742, compound

Product 1

HCID 131713848Hydrazinecarboxylic acid, 2-(2,5-diamino-1,5-dioxopentyl)-, 1,1-dimethylethyl ester, (S)-

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

7.00 Grams of Z-Gln-NHNHBoc was dissolved in 50 ml of methanol and was catallytically reduced by using palladium as the catalyst to obtain H-Gln-NHNHBoc.

Sources & evidence

ORD record
ord-1135f5e258f74faa9d3359a9bbb3106a
Source dataset
uspto-grants-1984_10
Patent number
US04474754

Reaction notes

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