HCID 13372703, compound → HCID 131713849, compound

HRID 1632398Notes

Reaction equation

HRID 1632398 reaction equation
[N:1]1(C(OCC2C=CC=CC=2)=O)[CH2:25][CH2:24][CH2:23][C@H:2]1[C:3]([NH:5][C@H:6]([C:12]([NH:14][NH:15][C:16]([O:18][C:19]([CH3:22])([CH3:21])[CH3:20])=[O:17])=[O:13])[CH2:7][CH2:8][C:9](=[O:11])[NH2:10])=[O:4]>CO.[Pd]>[NH:1]1[CH2:25][CH2:24][CH2:23][C@H:2]1[C:3]([NH:5][C@H:6]([C:12]([NH:14][NH:15][C:16]([O:18][C:19]([CH3:20])([CH3:21])[CH3:22])=[O:17])=[O:13])[CH2:7][CH2:8][C:9](=[O:11])[NH2:10])=[O:4]

Participants

4

Reactant 1

HCID 13372703HCID 13372703, compound

Product 1

HCID 131713849HCID 131713849, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

5.50 Grams of Z-Pro-Gln-NHNHBoc was dissolved in 50 ml of methanol and was catalytically reduced by using palladium as the catalyst to obtain H-Pro-Gln-NHNHBoc.

Sources & evidence

ORD record
ord-3ce618bc460e4fbc9a5131dac46a1bb0
Source dataset
uspto-grants-1984_10
Patent number
US04474754

Reaction notes

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