HCID 131713851, compound → HCID 131713850, compound

HRID 1632399Notes

Reaction equation

HRID 1632399 reaction equation
[NH:1](C(OCC1C=CC=CC=1)=O)[C@H:2]([C:7]([N:9]1[CH2:33][CH2:32][CH2:31][C@H:10]1[C:11]([NH:13][C@H:14]([C:20]([NH:22][NH:23][C:24]([O:26][C:27]([CH3:30])([CH3:29])[CH3:28])=[O:25])=[O:21])[CH2:15][CH2:16][C:17](=[O:19])[NH2:18])=[O:12])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5]>CO.[Pd]>[NH2:1][C@H:2]([C:7]([N:9]1[CH2:33][CH2:32][CH2:31][C@H:10]1[C:11]([NH:13][C@H:14]([C:20]([NH:22][NH:23][C:24]([O:26][C:27]([CH3:29])([CH3:28])[CH3:30])=[O:25])=[O:21])[CH2:15][CH2:16][C:17](=[O:19])[NH2:18])=[O:12])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5]

Participants

4

Reactant 1

HCID 131713851HCID 131713851, compound

Product 1

HCID 131713850HCID 131713850, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

3.50 Grams of Z-Leu-Pro-Gln-NHNHBoc was dissolved in 50 ml of methanol and was catalytically reduced by using palladium as the catalyst to obtain H-Leu-Pro-Gln-NHNHBoc.

Sources & evidence

ORD record
ord-6231a747b26540bdb6a2148d5cd9334e
Source dataset
uspto-grants-1984_10
Patent number
US04474754

Reaction notes

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