HCID 15585619, compound → HCID 131713854, compound

HRID 1632401Notes

Reaction equation

HRID 1632401 reaction equation
[NH:1](C(OCC1C=CC=CC=1)=O)[C@H:2]([C:5]([NH:7][C@H:8]([C:13]([NH:15][C@H:16]([C:21]([N:23]1[CH2:47][CH2:46][CH2:45][C@H:24]1[C:25]([NH:27][C@H:28]([C:34]([NH:36][NH:37][C:38]([O:40][C:41]([CH3:44])([CH3:43])[CH3:42])=[O:39])=[O:35])[CH2:29][CH2:30][C:31](=[O:33])[NH2:32])=[O:26])=[O:22])[CH2:17][CH:18]([CH3:20])[CH3:19])=[O:14])[CH2:9][C:10](=[O:12])[OH:11])=[O:6])[CH2:3][OH:4]>CO.[Pd]>[NH2:1][C@H:2]([C:5]([NH:7][C@H:8]([C:13]([NH:15][C@H:16]([C:21]([N:23]1[CH2:47][CH2:46][CH2:45][C@H:24]1[C:25]([NH:27][C@H:28]([C:34]([NH:36][NH:37][C:38]([O:40][C:41]([CH3:43])([CH3:42])[CH3:44])=[O:39])=[O:35])[CH2:29][CH2:30][C:31](=[O:33])[NH2:32])=[O:26])=[O:22])[CH2:17][CH:18]([CH3:20])[CH3:19])=[O:14])[CH2:9][C:10](=[O:11])[OH:12])=[O:6])[CH2:3][OH:4]

Participants

4

Reactant 1

HCID 15585619HCID 15585619, compound

Product 1

HCID 131713854HCID 131713854, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

1.03 Grams of Z-Ser-Asp-Leu-Pro-Gln-NHNHBoc was dissolved in 50 ml of methanol and was catalytically reduced by using palladium as the catalyst to obtain H-Ser-Asp-Leu-Pro-Gln-NHNHBoc.

Sources & evidence

ORD record
ord-d89400ec97444f07837457788c8451d1
Source dataset
uspto-grants-1984_10
Patent number
US04474754

Reaction notes

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