Benzylamine → HCID 13361983, compound

HRID 1632604Notes

Reaction equation

HRID 1632604 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH:6]=O.[CH2:11]([NH2:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>CCOCC>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH:6]=[N:18][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 2

HCID 7504BenzylamineHCID 115693-Methoxybenzaldehyde

Product 1

HCID 13361983HCID 13361983, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A solution of 100 gm. of 3-methoxybenzaldehyde. 78.7 gm. of benzylamine, and 800 ml. of anhydrous ether was refluxed for 14 hours and then concentrated in vacuo to an oil. Distillation provided 144.3 gm. of clear oil, b.p. 152°-154° (1.2 Torr).

Workup

  1. concentrationconcentrated in vacuo to an oil
  2. distillationDistillation
  3. customprovided 144.3 gm

Sources & evidence

ORD record
ord-8e9a8009943a4a208ce56b59d868d24d
Source dataset
uspto-grants-1984_10
Patent number
US04476311

Reaction notes

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