HRID1632668

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3283

Diethyl Ether

C4H10O

HCID775715

1-(4-methoxyphenyl)-1H-indole

C15H13NO

PRODUCTS

生成物

HCID13339544

1-(4-Methoxyphenyl)-1,3-dihydro-2H-indol-2-one

C15H13NO2

PROCEDURE

实验过程

Omitting the final chromatography, but triturating the crude product three times with ether, 1-(4-methoxyphenyl)indole (18.1 g, 81 mmoles) was converted to title product, 12.0 g, m.p. 115°-117° C., pnmr/CDCl3 /TMS/delta: 3.65 (s, 2H), 3.8 (s, 3H), 6.6-7.4 (m, 8H).