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HRID1632743

反应详情

EQUATION

反应方程式

HRID 1632743 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC(C)COC(=O)Cl
HCID62365

Isobutyl chloroformate

C5H9ClO2

结构：NS(=O)(=O)c1ccc(S(=O)(=O)c2ccc(O)cc2)s1
HCID12736892

5-(4-hydroxyphenyl)sulfonylthiophene-2-sulfonamide

C10H9NO5S3

PRODUCTS

生成物

1
结构：CC(C)COC(=O)Oc1ccc(S(=O)(=O)c2ccc(S(N)(=O)=O)s2)cc1
HCID20442366

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

A solution of 5-[(4-hydroxyphenyl)sulfonyl]thiophene-2-sulfonamide (2.50 g; 0.00783 mole) in acetone (50 ml) at 0° was treated with triethylamine (0.87 g; 0.00861 mole) followed by isobutyl chloroformate (1.17 g; 0.00861 mole) dropwise, during 30 minutes at 0°-2°.