HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 131713935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Orcinol | HCID 10436 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Catalyst | Phosphorus oxychloride | HCID 24813 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131713935 | HCID 131713935 | — |
Reaction Steps
To a solution of 621 g. of 5-methylresorcinol in 1 l. of dioxane were added 530 g. of benzaldehyde and 30 g. of phosphorus oxychloride as a catalyst. The resulting mixture was reacted at room temperature for 24 hours and then poured into 5 l. of a cold water. There was obtained a pale brown powdery resin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04477553 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-7d86d1ad78fa43c38d9eee38f163cd45 |
| Source note | uspto-grants-1984_10 |