HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → 3-(2-nitroethenyl)-1-phenylindole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | 1-Phenyl-1H-indole-3-carbaldehyde | HCID 12377926 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3-(2-nitroethenyl)-1-phenylindole | HCID 622004 | — |
Reaction Steps
120 g 1-phenylindole-3-carboxaldehyde and 16.2 g ammonium acetate are heated under reflux in 406 ml nitromethane for 5 hours. The mixture is cooled, diluted with ether to give 3-(2-nitroethenyl)-1-phenylindole, m.p. 154°-155°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04478750 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-8e9b440b800d4652a96cbb38cdffdc6a |
| Source note | uspto-grants-1984_10 |