HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-(Benzyloxy)pyridin-2-yl)methanol → 3-(Benzyloxy)pyridine-2-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-(Benzyloxy)pyridin-2-yl)methanol | HCID 13217540 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-(Benzyloxy)pyridine-2-carbaldehyde | HCID 13374594 | — |
Reaction Steps
3-Benzyloxy-2-(hydroxymethyl)pyridine (35.1 grams; 0.16 mole) was dissolved in 1 liter of CHCl3. Manganese dioxide (174 grams; 2.0 moles) was added and the mixture refluxed for a period of five hours. The reaction mixture was filtered hot through celite, and the solvent removed from the filtrate to afford a brown liquid weighing 23.5 grams.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04478834 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-74da63afd928441ea8a4e9c51d873cbf |
| Source note | uspto-grants-1984_10 |