2-Propenoyl chloride, 3-(3,4,5-trimethoxyphenyl)-, (2E)- → HCID 54554619, compound

HRID 1632972Notes

Reaction equation

HRID 1632972 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:11]=[C:12]([O:16][CH3:17])[C:13]=1[O:14][CH3:15])[CH:6]=[CH:7][C:8](Cl)=[O:9].[CH2:18]([NH:22][C:23]([CH:25]([N:27]1[CH2:32][CH2:31][NH:30][CH2:29][CH2:28]1)[CH3:26])=[O:24])[CH2:19][CH2:20][CH3:21]>C(Cl)(Cl)Cl>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:11]=[C:12]([O:16][CH3:17])[C:13]=1[O:14][CH3:15])[CH:6]=[CH:7][C:8]([N:30]1[CH2:29][CH2:28][N:27]([CH:25]([C:23]([NH:22][CH2:18][CH2:19][CH2:20][CH3:21])=[O:24])[CH3:26])[CH2:32][CH2:31]1)=[O:9]

Participants

4

Reactant 2

HCID 1120942-Propenoyl chloride, 3-(3,4,5-trimethoxyphenyl)-, (2E)-HCID 20441628HCID 20441628, compound

Product 1

HCID 54554619HCID 54554619, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

7.23 g of 3,4,5-trimethoxycinnamoyl chloride is added with stirring at room temperature to a solution of 5.00 g of 1-[1-(butylaminocarbonyl)ethyl]piperazine in 80 ml of chloroform, and the resulting solution is stirred at room temperature for 15 minutes.

Sources & evidence

ORD record
ord-7e18d49c8dd04599aea66c763765c6b8
Source dataset
uspto-grants-1984_10
Patent number
US04478838

Reaction notes

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