Acetic Anhydride → HCID 13339914, compound

Participants

Reaction Steps

A mixture of 11 g (16.5 mmole) of 6-aminomethyl-2,4-bis(methylthio)pyrimidine and 75 ml of acetic anhydride was stirred at room temperature for 16 hours, then evaporated. The residue was isolated by filtration and washed with a small amount of methanol to provide white solid 6-acetylaminomethyl-2,4-bis(methylthio)pyrimidine. The structural assignment was supported by infrared spectral analysis.

Provenance & Evidence