Sodium methanethiolate → HCID 13377373, compound

HRID 1632992Notes

Reaction equation

HRID 1632992 reaction equation
Cl[C:2]1[N:7]2[C:8]([CH3:11])=[N:9][CH:10]=[C:6]2[CH:5]=[C:4]([Cl:12])[N:3]=1.[CH3:13][S-:14].[Na+]>>[Cl:12][C:4]1[N:3]=[C:2]([S:14][CH3:13])[N:7]2[C:8]([CH3:11])=[N:9][CH:10]=[C:6]2[CH:5]=1

Participants

3

Reactant 2

HCID 4378561Sodium methanethiolateHCID 133773425,7-Dichloro-3-methylimidazo[1,5-c]pyrimidine

Product 1

HCID 13377373HCID 13377373, compound

Procedure

Using the method of Example 53, 5,7-dichloro-3-methylimidazo[1,5-c]pyrimidine (from Example 35) was reacted with sodium methanethiolate to provide yellow solid 7-chloro-3-methyl-5-methylthioimidazo[1,5-c]pyrimidine, m.p. 153°-155° C. Analysis: Calculated for C8H8ClN3S: %C, 45.0; %H, 3.8; %N, 19.7; Found: %C, 44.8; %H, 3.5; %N, 19.7.

Sources & evidence

ORD record
ord-7092a73eff3c4b248e1a59675ab96c23
Source dataset
uspto-grants-1984_10
Patent number
US04478835

Reaction notes

Loading…