Ethanolamine → HCID 13043448, compound

HRID 1633008Notes

Reaction equation

HRID 1633008 reaction equation
[CH2:1]([S:8][C:9]1[C:14]2[N:15]=[C:16](OC3C=CC=CC=3)[N:17]=[C:18]([N:19]3[CH2:24][CH2:23][O:22][CH2:21][CH2:20]3)[C:13]=2[N:12]=[CH:11][N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:32][CH2:33][CH2:34][NH2:35]>>[CH2:1]([S:8][C:9]1[C:14]2[N:15]=[C:16]([NH:35][CH2:34][CH2:33][OH:32])[N:17]=[C:18]([N:19]3[CH2:20][CH2:21][O:22][CH2:23][CH2:24]3)[C:13]=2[N:12]=[CH:11][N:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 13043449HCID 13043449, compound

Product 1

HCID 13043448HCID 13043448, compound

Procedure

The same substance was also obtained in analogous manner by heating 8-benzylthio-4-morpholino-2-phenoxypyrimido[5,4-d]pyrimidine (melting point: 159°-161° C.) at 90° C. with 2-hydroxyethyl-amine.

Workup

  1. customThe same substance was also obtained in analogous manner

Sources & evidence

ORD record
ord-f997e8abdf614dabaa562ed6150a0fa8
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

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