Ethanolamine → HCID 13043605, compound

HRID 1633018Notes

Reaction equation

HRID 1633018 reaction equation
[NH2:1][C:2]1[C:7]2[N:8]=[C:9](Cl)[N:10]=[C:11]([N:12]3[CH2:17][CH2:16][S:15](=[O:18])[CH2:14][CH2:13]3)[C:6]=2[N:5]=[CH:4][N:3]=1.[OH:20][CH2:21][CH2:22][NH2:23]>>[NH2:1][C:2]1[C:7]2[N:8]=[C:9]([NH:23][CH2:22][CH2:21][OH:20])[N:10]=[C:11]([N:12]3[CH2:17][CH2:16][S:15](=[O:18])[CH2:14][CH2:13]3)[C:6]=2[N:5]=[CH:4][N:3]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 12816997HCID 12816997, compound

Product 1

HCID 13043605HCID 13043605, compound

Procedure

This compound was prepared analogous to Example 2 from 8-amino-2-chloro-4-(1-oxido-thiomorpholino)-pyrimido[5,4-d]pyrimidine (melting point: 270°-272° C.; decomposition) and 2-hydroxyethyl-amine.

Sources & evidence

ORD record
ord-fd85ced778664782982b74ef18d611da
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

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