Ethanolamine → HCID 13043475, compound

HRID 1633020Notes

Reaction equation

HRID 1633020 reaction equation
[CH2:1]([NH:8][C:9]1[C:14]2[N:15]=[C:16](Cl)[N:17]=[C:18]([N:19]3[CH2:24][CH2:23][S:22](=[O:26])(=[O:25])[CH2:21][CH2:20]3)[C:13]=2[N:12]=[CH:11][N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:28][CH2:29][CH2:30][NH2:31]>>[CH2:1]([NH:8][C:9]1[C:14]2[N:15]=[C:16]([NH:31][CH2:30][CH2:29][OH:28])[N:17]=[C:18]([N:19]3[CH2:24][CH2:23][S:22](=[O:26])(=[O:25])[CH2:21][CH2:20]3)[C:13]=2[N:12]=[CH:11][N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 12817013HCID 12817013, compound

Product 1

HCID 13043475HCID 13043475, compound

Procedure

This compound was prepared analogous to Example 2 from 8-benzylamino-2-chloro-4-(1,1-dioxido-thiomorpholino)pyrimido[5,4-d]pyrimidine (melting point: 213°-215° C.) and 2-hydroxyethyl-amine.

Sources & evidence

ORD record
ord-e6f8ad0bbbf042cda2104b2dc2bccfd3
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

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