Ethanolamine → HCID 13043493, compound

HRID 1633022Notes

Reaction equation

HRID 1633022 reaction equation
[CH2:1]([N:8]([CH2:27][CH2:28][CH2:29][CH3:30])[C:9]1[C:14]2[N:15]=[C:16](Cl)[N:17]=[C:18]([N:19]3[CH2:24][CH2:23][S:22](=[O:25])[CH2:21][CH2:20]3)[C:13]=2[N:12]=[CH:11][N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:31][CH2:32][CH2:33][NH2:34]>>[CH2:1]([N:8]([CH2:27][CH2:28][CH2:29][CH3:30])[C:9]1[C:14]2[N:15]=[C:16]([NH:34][CH2:33][CH2:32][OH:31])[N:17]=[C:18]([N:19]3[CH2:24][CH2:23][S:22](=[O:25])[CH2:21][CH2:20]3)[C:13]=2[N:12]=[CH:11][N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 12817023HCID 12817023, compound

Product 1

HCID 13043493HCID 13043493, compound

Procedure

This compound was prepared analogous to Example 2 from 8-(N-benzyl-butylamino)-2-chloro-4-(1-oxido-thiomorpholino)-pyrimido[5,4-d]pyrimidine (melting point: 153°-155° C.) and 2-hydroxyethyl-amine.

Sources & evidence

ORD record
ord-0336a7e0db88442687d8c7b99324977b
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

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