Ethanolamine → HCID 13043501, compound

HRID 1633027Notes

Reaction equation

HRID 1633027 reaction equation
Cl[C:2]1[N:3]=[C:4]([N:20]2[CH2:25][CH2:24][S:23](=[O:26])[CH2:22][CH2:21]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([N:12]([CH3:19])[C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)[C:6]=2[N:7]=1.[OH:27][CH2:28][CH2:29][NH2:30]>>[OH:27][CH2:28][CH2:29][NH:30][C:2]1[N:3]=[C:4]([N:20]2[CH2:21][CH2:22][S:23](=[O:26])[CH2:24][CH2:25]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([N:12]([CH3:19])[C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=3)[C:6]=2[N:7]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 12817027HCID 12817027, compound

Product 1

HCID 13043501HCID 13043501, compound

Procedure

This compound was prepared analogous to Example 2 from 2-chloro-8-(N-methyl-anilino)-4-(1-oxido-thiomorpholino)pyrimido[5,4-d]pyrimidine (melting point: 237°-239° C.) and 2-hydroxyethyl-amine.

Sources & evidence

ORD record
ord-809dbe44a2494648b1348b30e5eddefb
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

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