Ethanolamine → HCID 13043502, compound

HRID 1633028Notes

Reaction equation

HRID 1633028 reaction equation
[CH2:1]([O:3][C:4]1[CH:28]=[CH:27][C:7]([NH:8][C:9]2[C:14]3[N:15]=[C:16](Cl)[N:17]=[C:18]([N:19]4[CH2:24][CH2:23][S:22](=[O:25])[CH2:21][CH2:20]4)[C:13]=3[N:12]=[CH:11][N:10]=2)=[CH:6][CH:5]=1)[CH3:2].[OH:29][CH2:30][CH2:31][NH2:32]>>[CH2:1]([O:3][C:4]1[CH:28]=[CH:27][C:7]([NH:8][C:9]2[C:14]3[N:15]=[C:16]([NH:32][CH2:31][CH2:30][OH:29])[N:17]=[C:18]([N:19]4[CH2:24][CH2:23][S:22](=[O:25])[CH2:21][CH2:20]4)[C:13]=3[N:12]=[CH:11][N:10]=2)=[CH:6][CH:5]=1)[CH3:2]

Participants

3

Reactant 2

HCID 700EthanolamineHCID 12817049HCID 12817049, compound

Product 1

HCID 13043502HCID 13043502, compound

Procedure

This compound was prepared analogous to Example 3 from 8-(4-ethoxy-anilino)-2-chloro-4-(1-oxido-thiomorpholino) pyrimido[5,4-d]pyrimidine (melting point: 237°-240° C.) and 2-hydroxyethyl-amine.

Sources & evidence

ORD record
ord-84274185787940358166be569403513b
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

Loading…