Ethanolamine → HCID 13043517, compound

HRID 1633030Notes

Reaction equation

HRID 1633030 reaction equation
Cl[C:2]1[N:3]=[C:4]([N:18]2[CH2:23][CH2:22][S:21](=[O:24])[CH2:20][CH2:19]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([N:12]3[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]3)[C:6]=2[N:7]=1.[OH:25][CH2:26][CH2:27][NH2:28]>>[OH:25][CH2:26][CH2:27][NH:28][C:2]1[N:3]=[C:4]([N:18]2[CH2:23][CH2:22][S:21](=[O:24])[CH2:20][CH2:19]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([N:12]3[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]3)[C:6]=2[N:7]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 12817007HCID 12817007, compound

Product 1

HCID 13043517HCID 13043517, compound

Procedure

This compound was prepared analogous to Example 3 from 2-chloro-4-(1-oxido-thiomorpholino)-8-piperidinopyrimido[5,4-d]pyrimidine (melting point: 203°-204° C.) and 2-hydroxyethyl-amine.

Sources & evidence

ORD record
ord-d5fe396812ba4439a2e81d8be55fbec3
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

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