Ethanolamine → HCID 13043523, compound

HRID 1633031Notes

Reaction equation

HRID 1633031 reaction equation
Cl[C:2]1[N:3]=[C:4]([N:17]2[CH2:22][CH2:21][S:20](=[O:23])[CH2:19][CH2:18]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([N:12]3[CH2:16][CH2:15][CH2:14][CH2:13]3)[C:6]=2[N:7]=1.[OH:24][CH2:25][CH2:26][NH2:27]>>[OH:24][CH2:25][CH2:26][NH:27][C:2]1[N:3]=[C:4]([N:17]2[CH2:22][CH2:21][S:20](=[O:23])[CH2:19][CH2:18]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([N:12]3[CH2:16][CH2:15][CH2:14][CH2:13]3)[C:6]=2[N:7]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 13043397HCID 13043397, compound

Product 1

HCID 13043523HCID 13043523, compound

Procedure

This compound was prepared analogous to Example 3 from 2-chloro-4-(1-oxido-thiomorpholino)-8-pyrrolidinopyrimido[5,4-d]pyrimidine (melting point: 243°-244° C.) and 2-hydroxyethyl-amine.

Sources & evidence

ORD record
ord-aea840bd446d471a854943fca73a0498
Source dataset
uspto-grants-1984_10
Patent number
US04478833

Reaction notes

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