HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 12582634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | HCID 178473320 | HCID 178473320 | — |
| Product | HCID 12582634 | HCID 12582634 | — |
Reaction Steps
A solution of 4.8 g of 5,6,7,8-tetrahydro-3-mercapto-6-pyrido[4,3-c]pyridazinecarboxylic acid ethyl ester in 20 cc of methylhydrazine is stirred at a bath temperature of 100° for 1 hour. The reaction solution is cooled with ice, and the precipitated reaction product is filtered off. The title compound has a M.P. of 121°-123° (decomp., from dimethoxyethane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04478837 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-7de227de63024b6e97005d168e5427e6 |
| Source note | uspto-grants-1984_10 |