Acetone → HCID 20441594, compound

HRID 1633068Notes

Reaction equation

HRID 1633068 reaction equation
[Cl:1][C:2]1[CH:21]=[CH:20][C:5]([C:6]([N:8]2[CH2:19][CH2:18][C:11]3[N:12]=[N:13][C:14]([NH:16][NH2:17])=[CH:15][C:10]=3[CH2:9]2)=[O:7])=[CH:4][CH:3]=1.[CH3:22][C:23]([CH3:25])=O>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([N:8]2[CH2:19][CH2:18][C:11]3[N:12]=[N:13][C:14]([NH:16][N:17]=[C:23]([CH3:25])[CH3:22])=[CH:15][C:10]=3[CH2:9]2)=[O:7])=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 180AcetoneHCID 20441582HCID 20441582, compound

Product 1

HCID 20441594HCID 20441594, compound

Procedure

A suspension of 3.1 g of crude 6-(p-chlorobenzoyl)-3-hydrazino-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine in 30 cc of acetone is heated on a water bath for 1 hour. The title compound has a M.P. of 221°-223° (decomp., from ethanol).

Workup

  1. temperatureis heated on a water bath for 1 hour

Sources & evidence

ORD record
ord-894e80abf2274260a746aab82d23b74f
Source dataset
uspto-grants-1984_10
Patent number
US04478837

Reaction notes

Loading…