Acetone → HCID 12582696, compound

HRID 1633069Notes

Reaction equation

HRID 1633069 reaction equation
[C:1]1([CH:7]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[CH2:8][C:9]([N:11]2[CH2:22][CH2:21][C:14]3[N:15]=[N:16][C:17]([NH:19][NH2:20])=[CH:18][C:13]=3[CH2:12]2)=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:29][C:30]([CH3:32])=O>>[C:23]1([CH:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH2:8][C:9]([N:11]2[CH2:22][CH2:21][C:14]3[N:15]=[N:16][C:17]([NH:19][N:20]=[C:30]([CH3:32])[CH3:29])=[CH:18][C:13]=3[CH2:12]2)=[O:10])[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 180AcetoneHCID 12582695HCID 12582695, compound

Product 1

HCID 12582696HCID 12582696, compound

Procedure

A solution of 1.5 g of 6-(3,3-diphenylpropionyl)-3-hydrazino-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine in 40 cc of absolute acetone is heated on a water bath for 35 minutes. The title compound has a M.P. of 172°-175° (decomp., from absolute ethanol).

Sources & evidence

ORD record
ord-d7457aea452e41b691e3303c24119bdd
Source dataset
uspto-grants-1984_10
Patent number
US04478837

Reaction notes

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