Acetone → HCID 20441627, compound

HRID 1633072Notes

Reaction equation

HRID 1633072 reaction equation
[C:1]([N:6]1[CH2:17][CH2:16][C:9]2[N:10]=[N:11][C:12]([NH:14][NH2:15])=[CH:13][C:8]=2[CH2:7]1)(=[O:5])[CH2:2][CH2:3][CH3:4].[CH3:18][C:19]([CH3:21])=O>>[C:1]([N:6]1[CH2:17][CH2:16][C:9]2[N:10]=[N:11][C:12]([NH:14][N:15]=[C:19]([CH3:21])[CH3:18])=[CH:13][C:8]=2[CH2:7]1)(=[O:5])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 180AcetoneHCID 12582639HCID 12582639, compound

Product 1

HCID 20441627HCID 20441627, compound

Procedure

A solution of 3.5 g of crude oily 6-butyryl-3-hydrazino-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine in 20 cc of acetone is heated to the boil at reflux on a water bath for 20 minutes. The title compound has a M.P. of 152°-154° (decomp., from acetone).

Workup

  1. temperatureat reflux on a water bath for 20 minutes

Sources & evidence

ORD record
ord-a8d82551870c44e0b7e2adf2e1f7f68b
Source dataset
uspto-grants-1984_10
Patent number
US04478837

Reaction notes

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