Acetone → HCID 20441545, compound

HRID 1633073Notes

Reaction equation

HRID 1633073 reaction equation
[NH:1]([C:3]1[N:8]=[N:7][C:6]2[CH2:9][CH2:10][N:11]([C:13](=[O:21])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH2:12][C:5]=2[CH:4]=1)[NH2:2].[CH3:22][C:23]([CH3:25])=O>>[C:23](=[N:2][NH:1][C:3]1[N:8]=[N:7][C:6]2[CH2:9][CH2:10][N:11]([C:13](=[O:21])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH2:12][C:5]=2[CH:4]=1)([CH3:25])[CH3:22]

Participants

3

Reactant 2

HCID 180AcetoneHCID 12582647HCID 12582647, compound

Product 1

HCID 20441545HCID 20441545, compound

Procedure

A solution of 3.5 g of crude semicrystalline 3-hydrazino-6-octanoyl-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine in 50 cc of acetone is heated to the boil at reflux while stirring for 30 minutes. The title compound has a M.P. of 118°-121° (decomp., from light gasoline).

Workup

  1. temperatureat reflux

Sources & evidence

ORD record
ord-302735674001479a8c26eaddb4f93fae
Source dataset
uspto-grants-1984_10
Patent number
US04478837

Reaction notes

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