Acetone → HCID 12582667, compound

HRID 1633078Notes

Reaction equation

HRID 1633078 reaction equation
[F:1][C:2]1[CH:21]=[CH:20][CH:19]=[CH:18][C:3]=1[C:4]([N:6]1[CH2:17][CH2:16][C:9]2[N:10]=[N:11][C:12]([NH:14][NH2:15])=[CH:13][C:8]=2[CH2:7]1)=[O:5].[CH3:22][C:23]([CH3:25])=O>>[F:1][C:2]1[CH:21]=[CH:20][CH:19]=[CH:18][C:3]=1[C:4]([N:6]1[CH2:17][CH2:16][C:9]2[N:10]=[N:11][C:12]([NH:14][N:15]=[C:23]([CH3:25])[CH3:22])=[CH:13][C:8]=2[CH2:7]1)=[O:5]

Participants

3

Reactant 2

HCID 180AcetoneHCID 12582666HCID 12582666, compound

Product 1

HCID 12582667HCID 12582667, compound

Procedure

1.0 g of 6-(o-fluorobenzoyl)-3-hydrazino-5,6,7,8-tetrahydropyrido[4,3-c]pyridazine is heated in 10 cc of acetone on a water bath at reflux for 30 minutes. The title compound has a M.P. of 200°-203° (decomp., from absolute ethanol).

Workup

  1. temperatureat reflux for 30 minutes

Sources & evidence

ORD record
ord-14d301e0bfe347c6b0bad3db18c16f4c
Source dataset
uspto-grants-1984_10
Patent number
US04478837

Reaction notes

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