Acetone → HCID 12582747, compound

HRID 1633082Notes

Reaction equation

HRID 1633082 reaction equation
[NH:1]([C:3]1[N:8]=[N:7][C:6]2[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:5]=2[CH:4]=1)[NH2:2].[CH3:15][C:16]([CH3:18])=O>>[C:16](=[N:2][NH:1][C:3]1[N:8]=[N:7][C:6]2[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:5]=2[CH:4]=1)([CH3:18])[CH3:15]

Participants

3

Reactant 2

HCID 180AcetoneHCID 12582745HCID 12582745, compound

Product 1

HCID 12582747HCID 12582747, compound

Procedure

A solution of 0.5 g of 3-hydrazino-5,6,7,8,9,10-hexahydrocycloocta[c]pyridazine in 15 cc of absolute acetone is heated on a water bath for 1 hour. After cooling the title compound crystallizes.

Sources & evidence

ORD record
ord-efc0aa4a0a354e1b8d546bfcc0426b18
Source dataset
uspto-grants-1984_10
Patent number
US04478837

Reaction notes

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