HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13894227, compound → beta-Damascenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13894227 | HCID 13894227 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | beta-Damascenone | HCID 5366074 | 80% |
Reaction Steps
11.6 g (0.05M) of 2,6,6-trimethyl-1-[4-hydroxy-hepta-1,6-dien-4-yl]-cyclohexa-1,3-diene were treated as indicated in the preceding example with 8.6 g (0.075M) of potassium tert-butoxide in 50 ml of DMF. β-Damascenone was obtained in 80% yield (7.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04479011 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-ba3422abe8274cb5939961888eb8dd83 |
| Source note | uspto-grants-1984_10 |