Fumaronitrile → 4'-Butoxy-4-methyl[1,1'-biphenyl]-2,3-dicarbonitrile

HRID 1633198Notes

Reaction equation

HRID 1633198 reaction equation
[CH2:1]([O:5][C:6]1[CH:11]=[CH:10][C:9]([CH:12]=[CH:13][CH:14]=[CH:15][CH3:16])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH3:4].[C:17](#[N:22])/[CH:18]=[CH:19]/[C:20]#[N:21]>>[CH2:1]([O:5][C:6]1[CH:7]=[CH:8][C:9]([C:12]2[CH:13]=[CH:14][C:15]([CH3:16])=[C:19]([C:20]#[N:21])[C:18]=2[C:17]#[N:22])=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 637930FumaronitrileHCID 543184001-Butoxy-4-(penta-1,3-dien-1-yl)benzene

Product 1

HCID 204397954'-Butoxy-4-methyl[1,1'-biphenyl]-2,3-dicarbonitrile

Procedure

Using 1-(p-n-butoxyphenyl)-4-methyl-1,3-butadiene and fumaronitrile, 3-(p-n-butoxyphenyl)-6-methylphthalonitrile was obtained by the same method as in Example 1. m.p. was 151.5° C.

Sources & evidence

ORD record
ord-54328306257e4caaab847919e3db3141
Source dataset
uspto-grants-1984_10
Patent number
US04479885

Reaction notes

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