Fumaronitrile → HCID 178450099, compound

HRID 1633199Notes

Reaction equation

[CH2:1]([C@H:4]1[CH2:9][CH2:8][C@H:7]([CH:10]=[CH:11][CH:12]=[CH:13][C:14]2[CH:19]=[CH:18][C:17]([O:20][CH2:21][CH2:22][CH2:23][CH3:24])=[CH:16][CH:15]=2)[CH2:6][CH2:5]1)[CH2:2][CH3:3].[C:25](#[N:30])/[CH:26]=[CH:27]/[C:28]#[N:29]>>[CH2:1]([C@H:4]1[CH2:5][CH2:6][C@H:7]([C:10]2[CH:11]=[CH:12][C:13]([C:14]3[CH:15]=[CH:16][C:17]([O:20][CH2:21][CH2:22][CH2:23][CH3:24])=[CH:18][CH:19]=3)=[C:27]([C:28]#[N:29])[C:26]=2[C:25]#[N:30])[CH2:8][CH2:9]1)[CH2:2][CH3:3]

Participants

Reactant 2

HCID 637930Fumaronitrile

HCID 178450141HCID 178450141, compound

Product 1

HCID 178450099HCID 178450099, compound

Procedure

Using 1-(Trans-4'-n-propylcyclohexyl)-4-(p-n-butoxyphenyl)-1,3-butadiene and fumaronitrile, 3-(trans-4'-n-propylcyclohexyl)-6-(p-n-butoxyphenyl)phthalonitrile was obtained by the same method as in Example 1. m.p. was 115° C.

Sources & evidence

ORD record: ord-93d521ab37a74e418a81bb6ce7a788e4
Source dataset: uspto-grants-1984_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04479885

Reaction notes

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