Fumaronitrile → HCID 178444283, compound

HRID 1633201Notes

Reaction equation

[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[CH:9][CH:10]=[CH:11][C@H:12]2[CH2:17][CH2:16][C@H:15]([CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:14][CH2:13]2)=[CH:4][CH:3]=1.[C:23](#[N:28])/[CH:24]=[CH:25]/[C:26]#[N:27]>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:9]=[CH:10][C:11]([C@H:12]3[CH2:13][CH2:14][C@H:15]([CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:16][CH2:17]3)=[C:25]([C:26]#[N:27])[C:24]=2[C:23]#[N:28])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 637930Fumaronitrile

HCID 178444447HCID 178444447, compound

Product 1

HCID 178444283HCID 178444283, compound

Procedure

Using 1-(p-fluorophenyl)-4-(trans-4'-n-pentylcyclohexyl)-1,3-butadiene and fumaronitrile, 3-(p-fluorophenyl)-6-(trans-4'-n-pentylcyclohexyl)phthalonitrile was obtained by the same method as in Example 1. m.p. was 102.5° C.

Sources & evidence

ORD record: ord-25e223b0c0d6461d99537dcd58bd0ad1
Source dataset: uspto-grants-1984_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04479885

Reaction notes

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